摘要
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Cobalt and chromium doped ferro spinels synthesized by sol-gel auto-combustion method with glycine as a fuel, calcination temperature of samples confirmed from TGA/DSC analysis. The observed elemental analysis from EDAX is in good...
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Cobalt and chromium doped ferro spinels synthesized by sol-gel auto-combustion method with glycine as a fuel, calcination temperature of samples confirmed from TGA/DSC analysis. The observed elemental analysis from EDAX is in good agreement with the theoretical composition of elements. The XRD and Rietveld analysis of XRD patterns illustrate formation of single- phase cubic spinel structure. The IR spectra shows two principle absorption bands. SEM and TEM images reveal well-defined nanoparticles with slight agglomeration. Calculated and observed magneton number decreased with Co2+ and Cr3+ substitution. 1, 8-dioxodecahydroacridines synthesized using synthesized ferrite nanoparticles as a catalyst.
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